Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling
ABSTRACT: Commercial powders of pure magnesium were processed by high-energy ball milling. The microstructural and morphological evolution of the powders was studied using scanning electron microscopy (SEM), energy dispersive spectrometry (EDX) and X-ray diffraction (XRD). From the results obtained,...
- Autores:
-
Ríos Arbeláez, Jesús María
Restrepo Carvajal, Alex Humberto
Zuleta Gil, Alejandro Alberto
Bolívar Osorio, Francisco Javier
Castaño González, Juan Guillermo
Correa Bedoya, Esteban Alberto
Echeverría Echeverría, Félix
- Tipo de recurso:
- Article of investigation
- Fecha de publicación:
- 2021
- Institución:
- Universidad de Antioquia
- Repositorio:
- Repositorio UdeA
- Idioma:
- eng
- OAI Identifier:
- oai:bibliotecadigital.udea.edu.co:10495/23199
- Acceso en línea:
- http://hdl.handle.net/10495/23199
- Palabra clave:
- Microestructura
Microstructure
Recristalización (metalurgia)
Recrystallization (Metallurgy)
Milling parameters
Morphological changes
Magnesium powders
- Rights
- openAccess
- License
- https://creativecommons.org/licenses/by/4.0/
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| dc.title.spa.fl_str_mv |
Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling |
| title |
Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling |
| spellingShingle |
Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling Microestructura Microstructure Recristalización (metalurgia) Recrystallization (Metallurgy) Milling parameters Morphological changes Magnesium powders |
| title_short |
Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling |
| title_full |
Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling |
| title_fullStr |
Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling |
| title_full_unstemmed |
Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling |
| title_sort |
Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling |
| dc.creator.fl_str_mv |
Ríos Arbeláez, Jesús María Restrepo Carvajal, Alex Humberto Zuleta Gil, Alejandro Alberto Bolívar Osorio, Francisco Javier Castaño González, Juan Guillermo Correa Bedoya, Esteban Alberto Echeverría Echeverría, Félix |
| dc.contributor.author.none.fl_str_mv |
Ríos Arbeláez, Jesús María Restrepo Carvajal, Alex Humberto Zuleta Gil, Alejandro Alberto Bolívar Osorio, Francisco Javier Castaño González, Juan Guillermo Correa Bedoya, Esteban Alberto Echeverría Echeverría, Félix |
| dc.contributor.researchgroup.spa.fl_str_mv |
Centro de Investigación Innovación y Desarrollo de Materiales (CIDEMAT) |
| dc.subject.lemb.none.fl_str_mv |
Microestructura Microstructure Recristalización (metalurgia) Recrystallization (Metallurgy) |
| topic |
Microestructura Microstructure Recristalización (metalurgia) Recrystallization (Metallurgy) Milling parameters Morphological changes Magnesium powders |
| dc.subject.proposal.spa.fl_str_mv |
Milling parameters Morphological changes Magnesium powders |
| description |
ABSTRACT: Commercial powders of pure magnesium were processed by high-energy ball milling. The microstructural and morphological evolution of the powders was studied using scanning electron microscopy (SEM), energy dispersive spectrometry (EDX) and X-ray diffraction (XRD). From the results obtained, it was determined that the ball size is the most influential milling parameter. This was because balls of 1 mm diameter were used after a previous stage of milling with larger balls (i.e., 10 and 3 mm). The powder particles presented an unusual morphology with respect to those observed in the Mg-milling literature and recrystallization phenomena. Moreover, the result strongly varied depending on the ball-to-powder weight ratio (BPR) used during the milling process. |
| publishDate |
2021 |
| dc.date.accessioned.none.fl_str_mv |
2021-10-14T17:46:26Z |
| dc.date.available.none.fl_str_mv |
2021-10-14T17:46:26Z |
| dc.date.issued.none.fl_str_mv |
2021 |
| dc.type.spa.fl_str_mv |
Artículo de investigación |
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http://purl.org/coar/resource_type/c_2df8fbb1 |
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https://purl.org/redcol/resource_type/ART |
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http://purl.org/coar/version/c_970fb48d4fbd8a85 |
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info:eu-repo/semantics/article |
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info:eu-repo/semantics/publishedVersion |
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http://purl.org/coar/resource_type/c_2df8fbb1 |
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publishedVersion |
| dc.identifier.citation.spa.fl_str_mv |
Rios, J.; Restrepo, A.; Zuleta, A.; Bolívar, F.; Castaño, J.; Correa, E.; Echeverria, F. Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling. Metals 2021, 11, 1621. https://doi.org/10.3390/ met11101621 |
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http://hdl.handle.net/10495/23199 |
| dc.identifier.doi.none.fl_str_mv |
10.3390/met11101621 |
| dc.identifier.eissn.none.fl_str_mv |
2075-4701 |
| identifier_str_mv |
Rios, J.; Restrepo, A.; Zuleta, A.; Bolívar, F.; Castaño, J.; Correa, E.; Echeverria, F. Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling. Metals 2021, 11, 1621. https://doi.org/10.3390/ met11101621 10.3390/met11101621 2075-4701 |
| url |
http://hdl.handle.net/10495/23199 |
| dc.language.iso.spa.fl_str_mv |
eng |
| language |
eng |
| dc.relation.ispartofjournalabbrev.spa.fl_str_mv |
Metals |
| dc.relation.citationendpage.spa.fl_str_mv |
10 |
| dc.relation.citationissue.spa.fl_str_mv |
10 |
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1 |
| dc.relation.citationvolume.spa.fl_str_mv |
11 |
| dc.relation.ispartofjournal.spa.fl_str_mv |
Metals |
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https://creativecommons.org/licenses/by/4.0/ |
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http://creativecommons.org/licenses/by/2.5/co/ |
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openAccess |
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10 |
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application/pdf |
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MDPI |
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Basilea, Suiza |
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Universidad de Antioquia |
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Ríos Arbeláez, Jesús MaríaRestrepo Carvajal, Alex HumbertoZuleta Gil, Alejandro AlbertoBolívar Osorio, Francisco JavierCastaño González, Juan GuillermoCorrea Bedoya, Esteban AlbertoEcheverría Echeverría, FélixCentro de Investigación Innovación y Desarrollo de Materiales (CIDEMAT)2021-10-14T17:46:26Z2021-10-14T17:46:26Z2021Rios, J.; Restrepo, A.; Zuleta, A.; Bolívar, F.; Castaño, J.; Correa, E.; Echeverria, F. Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball Milling. Metals 2021, 11, 1621. https://doi.org/10.3390/ met11101621http://hdl.handle.net/10495/2319910.3390/met111016212075-4701ABSTRACT: Commercial powders of pure magnesium were processed by high-energy ball milling. The microstructural and morphological evolution of the powders was studied using scanning electron microscopy (SEM), energy dispersive spectrometry (EDX) and X-ray diffraction (XRD). From the results obtained, it was determined that the ball size is the most influential milling parameter. This was because balls of 1 mm diameter were used after a previous stage of milling with larger balls (i.e., 10 and 3 mm). The powder particles presented an unusual morphology with respect to those observed in the Mg-milling literature and recrystallization phenomena. Moreover, the result strongly varied depending on the ball-to-powder weight ratio (BPR) used during the milling process.Departamento Administrativo de Ciencia, Tecnología e Innovación, MincienciasCOL000792710application/pdfengMDPIBasilea, Suizahttps://creativecommons.org/licenses/by/4.0/http://creativecommons.org/licenses/by/2.5/co/info:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_abf2Effect of Ball Size on the Microstructure and Morphology of Mg Powders Processed by High-Energy Ball MillingArtículo de investigaciónhttp://purl.org/coar/resource_type/c_2df8fbb1https://purl.org/redcol/resource_type/ARThttp://purl.org/coar/version/c_970fb48d4fbd8a85info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionMicroestructuraMicrostructureRecristalización (metalurgia)Recrystallization (Metallurgy)Milling parametersMorphological changesMagnesium powdersMetals1010111MetalsPrograma Nacional en IngenieríaObtención de nuevas aleaciones ligeras de alto valor agregado para contribuir al desarrollo de las industrias de biomateriales y aeronáuticas del país80740-183-2019PublicationORIGINALRiosJesus_2021_Effectball.pdfRiosJesus_2021_Effectball.pdfArtículo de investigaciónapplication/pdf2118460https://bibliotecadigital.udea.edu.co/bitstreams/4da7a316-2b37-44ad-a0a6-e0501f980a8b/download68e6348277820f6f16f3d5ab02dd1a4fMD51trueAnonymousREADCC-LICENSElicense_rdflicense_rdfapplication/rdf+xml; charset=utf-8927https://bibliotecadigital.udea.edu.co/bitstreams/482c42c7-2477-4c53-8c47-42a7ce250d44/download1646d1f6b96dbbbc38035efc9239ac9cMD52falseAnonymousREADLICENSElicense.txtlicense.txttext/plain; charset=utf-81748https://bibliotecadigital.udea.edu.co/bitstreams/bffbc9b2-d59e-4177-a0cb-2e23bce79b09/download8a4605be74aa9ea9d79846c1fba20a33MD53falseAnonymousREADTEXTRiosJesus_2021_Effectball.pdf.txtRiosJesus_2021_Effectball.pdf.txtExtracted texttext/plain47166https://bibliotecadigital.udea.edu.co/bitstreams/001ebc53-fdf5-4710-905b-455c9e47907e/download5ede8d15f518090e2c9510deafd3f4b1MD54falseAnonymousREADTHUMBNAILRiosJesus_2021_Effectball.pdf.jpgRiosJesus_2021_Effectball.pdf.jpgGenerated Thumbnailimage/jpeg16068https://bibliotecadigital.udea.edu.co/bitstreams/38894d8c-647f-461e-9be4-10b1d8b32e5d/download00e2a98cf1523f68001689e9d307d843MD55falseAnonymousREAD10495/23199oai:bibliotecadigital.udea.edu.co:10495/231992025-03-26 21:10:41.852https://creativecommons.org/licenses/by/4.0/open.accesshttps://bibliotecadigital.udea.edu.coRepositorio Institucional de la Universidad de Antioquiaaplicacionbibliotecadigitalbiblioteca@udea.edu.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 |