Design and implementation of an electrons detector in Mössbauer spectroscopy for reflection
A proportional detector for gas flow was designed, which can be applied to analyze both, bulk and thin films samples, using the Conversion Electron Mössbauer Spectroscopy technique (CEMS). The prototype is a stainless steel cylindrical chamber with extrusions for the input and output gas flow, condu...
- Autores:
- Tipo de recurso:
- Fecha de publicación:
- 2019
- Institución:
- Universidad Católica de Pereira
- Repositorio:
- Repositorio Institucional - RIBUC
- Idioma:
- spa
- OAI Identifier:
- oai:repositorio.ucp.edu.co:10785/9753
- Acceso en línea:
- https://revistas.ucp.edu.co/index.php/entrecienciaeingenieria/article/view/317
http://hdl.handle.net/10785/9753
- Palabra clave:
- Rights
- openAccess
- License
- Derechos de autor 2019 Entre Ciencia e Ingeniería
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Design and implementation of an electrons detector in Mössbauer spectroscopy for reflectionDiseño e implementación de un detector de electrones en espectroscopia Mössbauer por reflexiónDesenho e interpretação de um detector de elétrons em espectroscopia Mössbauer por reflexãoA proportional detector for gas flow was designed, which can be applied to analyze both, bulk and thin films samples, using the Conversion Electron Mössbauer Spectroscopy technique (CEMS). The prototype is a stainless steel cylindrical chamber with extrusions for the input and output gas flow, conductive strands and a sample holder which is bound to a micrometer, which allows to vary the distance between the sample and the copper strands. A gas mixture of 95% He + 5% CH4, which serves as signal multiplier gas and in turn controls the electron multiplication avoiding discharges that can damage the surface of the sample was used. The device was calibrated acquiring ICEMS spectrum for a sample containing iron, adjusting it with the MOSSFIT program, obtaining reported values from the hyperfine parameters.Se construyó un detector proporcional de flujo de gas para detectar electrones de la superficie de muestras en volumen y películas delgadas utilizando la técnica de Espectroscopia Mössbauer de electrones de conversión (CEMS). El prototipo es una cámara cilíndrica de acero inoxidable, con extrusiones para la entrada y salida de flujo de gas, filamentos conductores y un portamuestras que está unido a un tornillo micrómetrico el cual permite variar la distancia entre la muestra y los filamentos de cobre. Se usó una mezcla de gases, 95% He + 5% CH4, que cumple la función de gas multiplicador de la señal y a su vez controla la multiplicación de electrones los cuales pueden dañar la superficie de la muestra. El dispositivo fue calibrado adquiriendo el espectro ICEMS para una muestra con contenido de hierro, se realizó el ajuste de éste con el programa MOSFIT obteniendo valores reportados de los Parámetros Hiperfinos.Se construiu um detector proporcional de fluxo de gás para detectar elétrons da superfície de amostras em volume e películas finas utilizando a técnica de Espectroscopia Mössbauer de elétrons de conversão (CEMS). O protótipo é uma câmera cilíndrica de aço inoxidável, com extrusões para a entrada e saída de fluxo de gás, filamentos condutores e um porta amostras que está unido a um parafuso micrométrico o qual permite variar a distancia entre a amostra e os filamentos de cobre. Foi usado uma mescla de gases, 95% He+5% CH4, que cumpre a função de gás multiplicador do sinal e por sua vez controla a multiplicação de elétrons os quais podem danificar a superfície da amostra. O dispositivo foi calibrado adquirindo o espectro ICEMS para uma amostra com conteúdo de ferro, se realizou o ajuste deste com o programa MOSFIT obtendo valores informados dos Parâmetros Hiperfinos.Universidad Católica de Pereira2022-06-01T19:08:26Z2022-06-01T19:08:26Z2019-06-15Artículo de revistahttp://purl.org/coar/resource_type/c_6501http://purl.org/coar/version/c_970fb48d4fbd8a85info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionhttp://purl.org/coar/resource_type/c_2df8fbb1application/pdfhttps://revistas.ucp.edu.co/index.php/entrecienciaeingenieria/article/view/317http://hdl.handle.net/10785/9753Entre ciencia e ingeniería; Vol 10 No 20 (2016); 37-40Entre Ciencia e Ingeniería; Vol. 10 Núm. 20 (2016); 37-40Entre ciencia e ingeniería; v. 10 n. 20 (2016); 37-402539-41691909-8367spahttps://revistas.ucp.edu.co/index.php/entrecienciaeingenieria/article/view/317/307Derechos de autor 2019 Entre Ciencia e Ingenieríahttps://creativecommons.org/licenses/by-nc/4.0/deed.es_EShttps://creativecommons.org/licenses/by-nc/4.0/deed.es_ESinfo:eu-repo/semantics/openAccesshttp://purl.org/coar/access_right/c_abf2Cruz Muñoz, BeatrizGil Monsalve, KhaterineMedina, Milton HumbertoOsorio, Jaime Albertooai:repositorio.ucp.edu.co:10785/97532025-01-28T00:00:36Z |
| dc.title.none.fl_str_mv |
Design and implementation of an electrons detector in Mössbauer spectroscopy for reflection Diseño e implementación de un detector de electrones en espectroscopia Mössbauer por reflexión Desenho e interpretação de um detector de elétrons em espectroscopia Mössbauer por reflexão |
| title |
Design and implementation of an electrons detector in Mössbauer spectroscopy for reflection |
| spellingShingle |
Design and implementation of an electrons detector in Mössbauer spectroscopy for reflection |
| title_short |
Design and implementation of an electrons detector in Mössbauer spectroscopy for reflection |
| title_full |
Design and implementation of an electrons detector in Mössbauer spectroscopy for reflection |
| title_fullStr |
Design and implementation of an electrons detector in Mössbauer spectroscopy for reflection |
| title_full_unstemmed |
Design and implementation of an electrons detector in Mössbauer spectroscopy for reflection |
| title_sort |
Design and implementation of an electrons detector in Mössbauer spectroscopy for reflection |
| description |
A proportional detector for gas flow was designed, which can be applied to analyze both, bulk and thin films samples, using the Conversion Electron Mössbauer Spectroscopy technique (CEMS). The prototype is a stainless steel cylindrical chamber with extrusions for the input and output gas flow, conductive strands and a sample holder which is bound to a micrometer, which allows to vary the distance between the sample and the copper strands. A gas mixture of 95% He + 5% CH4, which serves as signal multiplier gas and in turn controls the electron multiplication avoiding discharges that can damage the surface of the sample was used. The device was calibrated acquiring ICEMS spectrum for a sample containing iron, adjusting it with the MOSSFIT program, obtaining reported values from the hyperfine parameters. |
| publishDate |
2019 |
| dc.date.none.fl_str_mv |
2019-06-15 2022-06-01T19:08:26Z 2022-06-01T19:08:26Z |
| dc.type.none.fl_str_mv |
Artículo de revista http://purl.org/coar/resource_type/c_6501 http://purl.org/coar/version/c_970fb48d4fbd8a85 info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion |
| dc.type.coar.fl_str_mv |
http://purl.org/coar/resource_type/c_2df8fbb1 |
| status_str |
publishedVersion |
| dc.identifier.none.fl_str_mv |
https://revistas.ucp.edu.co/index.php/entrecienciaeingenieria/article/view/317 http://hdl.handle.net/10785/9753 |
| url |
https://revistas.ucp.edu.co/index.php/entrecienciaeingenieria/article/view/317 http://hdl.handle.net/10785/9753 |
| dc.language.none.fl_str_mv |
spa |
| language |
spa |
| dc.relation.none.fl_str_mv |
https://revistas.ucp.edu.co/index.php/entrecienciaeingenieria/article/view/317/307 |
| dc.rights.none.fl_str_mv |
Derechos de autor 2019 Entre Ciencia e Ingeniería https://creativecommons.org/licenses/by-nc/4.0/deed.es_ES https://creativecommons.org/licenses/by-nc/4.0/deed.es_ES info:eu-repo/semantics/openAccess http://purl.org/coar/access_right/c_abf2 |
| rights_invalid_str_mv |
Derechos de autor 2019 Entre Ciencia e Ingeniería https://creativecommons.org/licenses/by-nc/4.0/deed.es_ES http://purl.org/coar/access_right/c_abf2 |
| eu_rights_str_mv |
openAccess |
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application/pdf |
| dc.publisher.none.fl_str_mv |
Universidad Católica de Pereira |
| publisher.none.fl_str_mv |
Universidad Católica de Pereira |
| dc.source.none.fl_str_mv |
Entre ciencia e ingeniería; Vol 10 No 20 (2016); 37-40 Entre Ciencia e Ingeniería; Vol. 10 Núm. 20 (2016); 37-40 Entre ciencia e ingeniería; v. 10 n. 20 (2016); 37-40 2539-4169 1909-8367 |
| institution |
Universidad Católica de Pereira |
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1844494680788566016 |