Synthesis and characterization of Pr2S3 binary compound
1 recurso en línea (páginas 95-98).
- Autores:
- Tipo de recurso:
- article
- Fecha de publicación:
- 2018
- Institución:
- Universidad Pedagógica y Tecnológica de Colombia
- Repositorio:
- RiUPTC: Repositorio Institucional UPTC
- Idioma:
- eng
- OAI Identifier:
- oai:repositorio.uptc.edu.co:001/2367
- Acceso en línea:
- http://repositorio.uptc.edu.co/handle/001/2367
- Palabra clave:
- Tratamiento con praseodimio
Tratamiento térmico
Semiconductor
- Rights
- openAccess
- License
- Copyright (c) 2018 Universidad Pedagógica y Tecnológica de Colombia
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Synthesis and characterization of Pr2S3 binary compoundSíntesis y caracterización del compuesto binario Pr2S3Quijano Ortega, NataliaGaona Jurado, SoniaRamírez Sanabria, Alfonso EnriqueTratamiento con praseodimioTratamiento térmicoSemiconductor1 recurso en línea (páginas 95-98).In the current work it is shown that the synthesis method that consists in direct reaction of praseodymium and sulfur in its elemental form, using heat as a treatment, with relatively low temperatures and reaction time of one week, allows the preparation of Pr2S3 compound, with a purity of about 92%. The respective characterization of resultant materials was carried out using powder XRD, where by it was determined that the thermal treatment used, effectively leads to the binary sulfide of interest, a compound known to be semiconductor.En el trabajo actual se muestra que el método de síntesis que consiste en la reacción directa de praseodimio y azufre en su forma elemental, utiliza calor como tratamiento, con temperaturas relativamente bajas y tiempo de reacción de una semana, permite la preparación del compuesto Pr2S3, con una pureza de alrededor del 92%. La caracterización respectiva de los materiales resultantes se llevó a cabo utilizando polvo XRD, donde se determinó que el tratamiento térmico utilizado conduce de manera efectiva a la fuente binaria de interés, un compuesto conocido por ser semiconductor.Bibliografía: página 98.Universidad Pedagógica y Tecnológica de Colombia2019-01-31T20:42:40Z2019-01-31T20:42:40Z2018-07-04Artículo de revistahttp://purl.org/coar/resource_type/c_6501info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionTexthttps://purl.org/redcol/resource_type/ARThttp://purl.org/coar/version/c_970fb48d4fbd8a85application/pdfapplication/pdfQuijano Ortega, N., Gaona Jurado, S. & Ramírez Sanabria, A. E. (2018). Synthesis and characterization of Pr2S3 binary compound. Ciencia en Desarrollo, 9(2), 95-98. DOI: https://doi.org/10.19053/01217488.v9.n2.2018.5974. http://repositorio.uptc.edu.co/handle/001/23672462-7658http://repositorio.uptc.edu.co/handle/001/236710.19053/01217488.v9.n2.2018.5974https://revistas.uptc.edu.co/index.php/ciencia_en_desarrollo/article/view/5974/7262reponame:RiUPTC: Repositorio Institucional UPTCinstname:Universidad Pedagógica y Tecnológica de Colombiainstacron:Universidad Pedagógica y Tecnológica de ColombiaengSelishchev, A. and V. Pavlishchuk, Effect of Formation Conditions on the Size, Shape and Spectral Properties of EuS and Pr2S3 Nanoparticles. Theoretical and Experimental Chemistry, 2014. 50(1): p. 39-45.Krichevtsov, B., Anisotropy of the linear and quadratic magnetic birefringence in rare-earth semiconductors (γ-Ln2S3 (Ln= Dy3+, Pr3+, Gd3+, La3+). Journal of Experimental and Theoretical Physics, 2001. 92(5): p. 830-839.Ohta, M., et al., Preparation of R2S3 (R: La, Pr, Nd, Sm) powders by sulfurization of oxide powders using CS2 gas. Journal of alloys and compounds, 2004. 374(1): p. 112-115.Ohta, M., et al., Phase transformation and microstructures of Ln2S3 (Ln= La, Sm) with different impurities content of oxygen and carbon. Journal of alloys and compounds, 2006. 408: p. 551-555.Ohta, M., et al., Thermoelectric properties of Th3P4-type rare-earth sulfides Ln2S3 (Ln= Gd, Tb) prepared by reaction of their oxides with CS2 gas. Journal of Alloys and Compounds, 2008. 451(1): p. 627-631.Ciencia en Desarrollo;Volumen 9, número 2 (Julio-Diciembre 2018)Copyright (c) 2018 Universidad Pedagógica y Tecnológica de Colombiahttps://creativecommons.org/licenses/by-nc/4.0/info:eu-repo/semantics/openAccessAtribución-NoComercial 4.0 Internacional (CC BY-NC 4.0)http://purl.org/coar/access_right/c_abf22021-02-10T13:03:17Z |
dc.title.none.fl_str_mv |
Synthesis and characterization of Pr2S3 binary compound Síntesis y caracterización del compuesto binario Pr2S3 |
title |
Synthesis and characterization of Pr2S3 binary compound |
spellingShingle |
Synthesis and characterization of Pr2S3 binary compound Quijano Ortega, Natalia Tratamiento con praseodimio Tratamiento térmico Semiconductor |
title_short |
Synthesis and characterization of Pr2S3 binary compound |
title_full |
Synthesis and characterization of Pr2S3 binary compound |
title_fullStr |
Synthesis and characterization of Pr2S3 binary compound |
title_full_unstemmed |
Synthesis and characterization of Pr2S3 binary compound |
title_sort |
Synthesis and characterization of Pr2S3 binary compound |
dc.creator.none.fl_str_mv |
Quijano Ortega, Natalia Gaona Jurado, Sonia Ramírez Sanabria, Alfonso Enrique |
author |
Quijano Ortega, Natalia |
author_facet |
Quijano Ortega, Natalia Gaona Jurado, Sonia Ramírez Sanabria, Alfonso Enrique |
author_role |
author |
author2 |
Gaona Jurado, Sonia Ramírez Sanabria, Alfonso Enrique |
author2_role |
author author |
dc.subject.none.fl_str_mv |
Tratamiento con praseodimio Tratamiento térmico Semiconductor |
topic |
Tratamiento con praseodimio Tratamiento térmico Semiconductor |
description |
1 recurso en línea (páginas 95-98). |
publishDate |
2018 |
dc.date.none.fl_str_mv |
2018-07-04 2019-01-31T20:42:40Z 2019-01-31T20:42:40Z |
dc.type.none.fl_str_mv |
Artículo de revista http://purl.org/coar/resource_type/c_6501 info:eu-repo/semantics/article info:eu-repo/semantics/publishedVersion Text https://purl.org/redcol/resource_type/ART http://purl.org/coar/version/c_970fb48d4fbd8a85 |
format |
article |
status_str |
publishedVersion |
dc.identifier.none.fl_str_mv |
Quijano Ortega, N., Gaona Jurado, S. & Ramírez Sanabria, A. E. (2018). Synthesis and characterization of Pr2S3 binary compound. Ciencia en Desarrollo, 9(2), 95-98. DOI: https://doi.org/10.19053/01217488.v9.n2.2018.5974. http://repositorio.uptc.edu.co/handle/001/2367 2462-7658 http://repositorio.uptc.edu.co/handle/001/2367 10.19053/01217488.v9.n2.2018.5974 |
identifier_str_mv |
Quijano Ortega, N., Gaona Jurado, S. & Ramírez Sanabria, A. E. (2018). Synthesis and characterization of Pr2S3 binary compound. Ciencia en Desarrollo, 9(2), 95-98. DOI: https://doi.org/10.19053/01217488.v9.n2.2018.5974. http://repositorio.uptc.edu.co/handle/001/2367 2462-7658 10.19053/01217488.v9.n2.2018.5974 |
url |
http://repositorio.uptc.edu.co/handle/001/2367 |
dc.language.none.fl_str_mv |
eng |
language |
eng |
dc.relation.none.fl_str_mv |
Selishchev, A. and V. Pavlishchuk, Effect of Formation Conditions on the Size, Shape and Spectral Properties of EuS and Pr2S3 Nanoparticles. Theoretical and Experimental Chemistry, 2014. 50(1): p. 39-45. Krichevtsov, B., Anisotropy of the linear and quadratic magnetic birefringence in rare-earth semiconductors (γ-Ln2S3 (Ln= Dy3+, Pr3+, Gd3+, La3+). Journal of Experimental and Theoretical Physics, 2001. 92(5): p. 830-839. Ohta, M., et al., Preparation of R2S3 (R: La, Pr, Nd, Sm) powders by sulfurization of oxide powders using CS2 gas. Journal of alloys and compounds, 2004. 374(1): p. 112-115. Ohta, M., et al., Phase transformation and microstructures of Ln2S3 (Ln= La, Sm) with different impurities content of oxygen and carbon. Journal of alloys and compounds, 2006. 408: p. 551-555. Ohta, M., et al., Thermoelectric properties of Th3P4-type rare-earth sulfides Ln2S3 (Ln= Gd, Tb) prepared by reaction of their oxides with CS2 gas. Journal of Alloys and Compounds, 2008. 451(1): p. 627-631. Ciencia en Desarrollo;Volumen 9, número 2 (Julio-Diciembre 2018) |
dc.rights.none.fl_str_mv |
Copyright (c) 2018 Universidad Pedagógica y Tecnológica de Colombia https://creativecommons.org/licenses/by-nc/4.0/ info:eu-repo/semantics/openAccess Atribución-NoComercial 4.0 Internacional (CC BY-NC 4.0) http://purl.org/coar/access_right/c_abf2 |
rights_invalid_str_mv |
Copyright (c) 2018 Universidad Pedagógica y Tecnológica de Colombia https://creativecommons.org/licenses/by-nc/4.0/ Atribución-NoComercial 4.0 Internacional (CC BY-NC 4.0) http://purl.org/coar/access_right/c_abf2 |
eu_rights_str_mv |
openAccess |
dc.format.none.fl_str_mv |
application/pdf application/pdf |
dc.publisher.none.fl_str_mv |
Universidad Pedagógica y Tecnológica de Colombia |
publisher.none.fl_str_mv |
Universidad Pedagógica y Tecnológica de Colombia |
dc.source.none.fl_str_mv |
https://revistas.uptc.edu.co/index.php/ciencia_en_desarrollo/article/view/5974/7262 reponame:RiUPTC: Repositorio Institucional UPTC instname:Universidad Pedagógica y Tecnológica de Colombia instacron:Universidad Pedagógica y Tecnológica de Colombia |
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Universidad Pedagógica y Tecnológica de Colombia |
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