Synthesis and characterization of Pr2S3 binary compound

1 recurso en línea (páginas 95-98).

Autores:
Tipo de recurso:
article
Fecha de publicación:
2018
Institución:
Universidad Pedagógica y Tecnológica de Colombia
Repositorio:
RiUPTC: Repositorio Institucional UPTC
Idioma:
eng
OAI Identifier:
oai:repositorio.uptc.edu.co:001/2367
Acceso en línea:
http://repositorio.uptc.edu.co/handle/001/2367
Palabra clave:
Tratamiento con praseodimio
Tratamiento térmico
Semiconductor
Rights
openAccess
License
Copyright (c) 2018 Universidad Pedagógica y Tecnológica de Colombia
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spelling Synthesis and characterization of Pr2S3 binary compoundSíntesis y caracterización del compuesto binario Pr2S3Quijano Ortega, NataliaGaona Jurado, SoniaRamírez Sanabria, Alfonso EnriqueTratamiento con praseodimioTratamiento térmicoSemiconductor1 recurso en línea (páginas 95-98).In the current work it is shown that the synthesis method that consists in direct reaction of praseodymium and sulfur in its elemental form, using heat as a treatment, with relatively low temperatures and reaction time of one week, allows the preparation of Pr2S3 compound, with a purity of about 92%. The respective characterization of resultant materials was carried out using powder XRD, where by it was determined that the thermal treatment used, effectively leads to the binary sulfide of interest, a compound known to be semiconductor.En el trabajo actual se muestra que el método de síntesis que consiste en la reacción directa de praseodimio y azufre en su forma elemental, utiliza calor como tratamiento, con temperaturas relativamente bajas y tiempo de reacción de una semana, permite la preparación del compuesto Pr2S3, con una pureza de alrededor del 92%. La caracterización respectiva de los materiales resultantes se llevó a cabo utilizando polvo XRD, donde se determinó que el tratamiento térmico utilizado conduce de manera efectiva a la fuente binaria de interés, un compuesto conocido por ser semiconductor.Bibliografía: página 98.Universidad Pedagógica y Tecnológica de Colombia2019-01-31T20:42:40Z2019-01-31T20:42:40Z2018-07-04Artículo de revistahttp://purl.org/coar/resource_type/c_6501info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersionTexthttps://purl.org/redcol/resource_type/ARThttp://purl.org/coar/version/c_970fb48d4fbd8a85application/pdfapplication/pdfQuijano Ortega, N., Gaona Jurado, S. & Ramírez Sanabria, A. E. (2018). Synthesis and characterization of Pr2S3 binary compound. Ciencia en Desarrollo, 9(2), 95-98. DOI: https://doi.org/10.19053/01217488.v9.n2.2018.5974. http://repositorio.uptc.edu.co/handle/001/23672462-7658http://repositorio.uptc.edu.co/handle/001/236710.19053/01217488.v9.n2.2018.5974https://revistas.uptc.edu.co/index.php/ciencia_en_desarrollo/article/view/5974/7262reponame:RiUPTC: Repositorio Institucional UPTCinstname:Universidad Pedagógica y Tecnológica de Colombiainstacron:Universidad Pedagógica y Tecnológica de ColombiaengSelishchev, A. and V. Pavlishchuk, Effect of Formation Conditions on the Size, Shape and Spectral Properties of EuS and Pr2S3 Nanoparticles. Theoretical and Experimental Chemistry, 2014. 50(1): p. 39-45.Krichevtsov, B., Anisotropy of the linear and quadratic magnetic birefringence in rare-earth semiconductors (γ-Ln2S3 (Ln= Dy3+, Pr3+, Gd3+, La3+). Journal of Experimental and Theoretical Physics, 2001. 92(5): p. 830-839.Ohta, M., et al., Preparation of R2S3 (R: La, Pr, Nd, Sm) powders by sulfurization of oxide powders using CS2 gas. Journal of alloys and compounds, 2004. 374(1): p. 112-115.Ohta, M., et al., Phase transformation and microstructures of Ln2S3 (Ln= La, Sm) with different impurities content of oxygen and carbon. Journal of alloys and compounds, 2006. 408: p. 551-555.Ohta, M., et al., Thermoelectric properties of Th3P4-type rare-earth sulfides Ln2S3 (Ln= Gd, Tb) prepared by reaction of their oxides with CS2 gas. Journal of Alloys and Compounds, 2008. 451(1): p. 627-631.Ciencia en Desarrollo;Volumen 9, número 2 (Julio-Diciembre 2018)Copyright (c) 2018 Universidad Pedagógica y Tecnológica de Colombiahttps://creativecommons.org/licenses/by-nc/4.0/info:eu-repo/semantics/openAccessAtribución-NoComercial 4.0 Internacional (CC BY-NC 4.0)http://purl.org/coar/access_right/c_abf22021-02-10T13:03:17Z
dc.title.none.fl_str_mv Synthesis and characterization of Pr2S3 binary compound
Síntesis y caracterización del compuesto binario Pr2S3
title Synthesis and characterization of Pr2S3 binary compound
spellingShingle Synthesis and characterization of Pr2S3 binary compound
Quijano Ortega, Natalia
Tratamiento con praseodimio
Tratamiento térmico
Semiconductor
title_short Synthesis and characterization of Pr2S3 binary compound
title_full Synthesis and characterization of Pr2S3 binary compound
title_fullStr Synthesis and characterization of Pr2S3 binary compound
title_full_unstemmed Synthesis and characterization of Pr2S3 binary compound
title_sort Synthesis and characterization of Pr2S3 binary compound
dc.creator.none.fl_str_mv Quijano Ortega, Natalia
Gaona Jurado, Sonia
Ramírez Sanabria, Alfonso Enrique
author Quijano Ortega, Natalia
author_facet Quijano Ortega, Natalia
Gaona Jurado, Sonia
Ramírez Sanabria, Alfonso Enrique
author_role author
author2 Gaona Jurado, Sonia
Ramírez Sanabria, Alfonso Enrique
author2_role author
author
dc.subject.none.fl_str_mv Tratamiento con praseodimio
Tratamiento térmico
Semiconductor
topic Tratamiento con praseodimio
Tratamiento térmico
Semiconductor
description 1 recurso en línea (páginas 95-98).
publishDate 2018
dc.date.none.fl_str_mv 2018-07-04
2019-01-31T20:42:40Z
2019-01-31T20:42:40Z
dc.type.none.fl_str_mv Artículo de revista
http://purl.org/coar/resource_type/c_6501
info:eu-repo/semantics/article
info:eu-repo/semantics/publishedVersion
Text
https://purl.org/redcol/resource_type/ART
http://purl.org/coar/version/c_970fb48d4fbd8a85
format article
status_str publishedVersion
dc.identifier.none.fl_str_mv Quijano Ortega, N., Gaona Jurado, S. & Ramírez Sanabria, A. E. (2018). Synthesis and characterization of Pr2S3 binary compound. Ciencia en Desarrollo, 9(2), 95-98. DOI: https://doi.org/10.19053/01217488.v9.n2.2018.5974. http://repositorio.uptc.edu.co/handle/001/2367
2462-7658
http://repositorio.uptc.edu.co/handle/001/2367
10.19053/01217488.v9.n2.2018.5974
identifier_str_mv Quijano Ortega, N., Gaona Jurado, S. & Ramírez Sanabria, A. E. (2018). Synthesis and characterization of Pr2S3 binary compound. Ciencia en Desarrollo, 9(2), 95-98. DOI: https://doi.org/10.19053/01217488.v9.n2.2018.5974. http://repositorio.uptc.edu.co/handle/001/2367
2462-7658
10.19053/01217488.v9.n2.2018.5974
url http://repositorio.uptc.edu.co/handle/001/2367
dc.language.none.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Selishchev, A. and V. Pavlishchuk, Effect of Formation Conditions on the Size, Shape and Spectral Properties of EuS and Pr2S3 Nanoparticles. Theoretical and Experimental Chemistry, 2014. 50(1): p. 39-45.
Krichevtsov, B., Anisotropy of the linear and quadratic magnetic birefringence in rare-earth semiconductors (γ-Ln2S3 (Ln= Dy3+, Pr3+, Gd3+, La3+). Journal of Experimental and Theoretical Physics, 2001. 92(5): p. 830-839.
Ohta, M., et al., Preparation of R2S3 (R: La, Pr, Nd, Sm) powders by sulfurization of oxide powders using CS2 gas. Journal of alloys and compounds, 2004. 374(1): p. 112-115.
Ohta, M., et al., Phase transformation and microstructures of Ln2S3 (Ln= La, Sm) with different impurities content of oxygen and carbon. Journal of alloys and compounds, 2006. 408: p. 551-555.
Ohta, M., et al., Thermoelectric properties of Th3P4-type rare-earth sulfides Ln2S3 (Ln= Gd, Tb) prepared by reaction of their oxides with CS2 gas. Journal of Alloys and Compounds, 2008. 451(1): p. 627-631.
Ciencia en Desarrollo;Volumen 9, número 2 (Julio-Diciembre 2018)
dc.rights.none.fl_str_mv Copyright (c) 2018 Universidad Pedagógica y Tecnológica de Colombia
https://creativecommons.org/licenses/by-nc/4.0/
info:eu-repo/semantics/openAccess
Atribución-NoComercial 4.0 Internacional (CC BY-NC 4.0)
http://purl.org/coar/access_right/c_abf2
rights_invalid_str_mv Copyright (c) 2018 Universidad Pedagógica y Tecnológica de Colombia
https://creativecommons.org/licenses/by-nc/4.0/
Atribución-NoComercial 4.0 Internacional (CC BY-NC 4.0)
http://purl.org/coar/access_right/c_abf2
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
application/pdf
dc.publisher.none.fl_str_mv Universidad Pedagógica y Tecnológica de Colombia
publisher.none.fl_str_mv Universidad Pedagógica y Tecnológica de Colombia
dc.source.none.fl_str_mv https://revistas.uptc.edu.co/index.php/ciencia_en_desarrollo/article/view/5974/7262
reponame:RiUPTC: Repositorio Institucional UPTC
instname:Universidad Pedagógica y Tecnológica de Colombia
instacron:Universidad Pedagógica y Tecnológica de Colombia
instname_str Universidad Pedagógica y Tecnológica de Colombia
instacron_str Universidad Pedagógica y Tecnológica de Colombia
institution Universidad Pedagógica y Tecnológica de Colombia
reponame_str RiUPTC: Repositorio Institucional UPTC
collection RiUPTC: Repositorio Institucional UPTC
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