Intervención didáctica para la extracción y cuantificación de esteroides en orina

Autores:: Angulo, Diego Hernando
Casas, Jaime Augusto
Cipagauta, Edna Carolina
Aparicio, David Eduardo

Tipo de recurso:: Article of journal

Fecha de publicación:: 2021

Institución:: Universidad Pedagógica y Tecnológica de Colombia

Repositorio:: RiUPTC: Repositorio Institucional UPTC

Idioma:

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dc.title.spa.fl_str_mv	Intervención didáctica para la extracción y cuantificación de esteroides en orina
title	Intervención didáctica para la extracción y cuantificación de esteroides en orina
spellingShingle	Intervención didáctica para la extracción y cuantificación de esteroides en orina Experimental science didactics Laboratory practical training Sample preparation SPE HPLC Didáctica de las ciencias experimentales Trabajos prácticos de laboratorio Preparación de muestras Didática das ciências experimentais Prática laboratorial Preparação de amostras
title_short	Intervención didáctica para la extracción y cuantificación de esteroides en orina
title_full	Intervención didáctica para la extracción y cuantificación de esteroides en orina
title_fullStr	Intervención didáctica para la extracción y cuantificación de esteroides en orina
title_full_unstemmed	Intervención didáctica para la extracción y cuantificación de esteroides en orina
title_sort	Intervención didáctica para la extracción y cuantificación de esteroides en orina
dc.creator.fl_str_mv	Angulo, Diego Hernando Casas, Jaime Augusto Cipagauta, Edna Carolina Aparicio, David Eduardo
dc.contributor.author.spa.fl_str_mv	Angulo, Diego Hernando Casas, Jaime Augusto Cipagauta, Edna Carolina Aparicio, David Eduardo
dc.subject.none.fl_str_mv	Experimental science didactics Laboratory practical training Sample preparation SPE HPLC Didáctica de las ciencias experimentales Trabajos prácticos de laboratorio Preparación de muestras Didática das ciências experimentais Prática laboratorial Preparação de amostras
topic	Experimental science didactics Laboratory practical training Sample preparation SPE HPLC Didáctica de las ciencias experimentales Trabajos prácticos de laboratorio Preparación de muestras Didática das ciências experimentais Prática laboratorial Preparação de amostras
publishDate	2021
dc.date.accessioned.none.fl_str_mv	2021-01-14 00:00:00 2026-04-16T17:39:47Z
dc.date.available.none.fl_str_mv	2021-01-14 00:00:00
dc.date.issued.none.fl_str_mv	2021-01-14
dc.type.spa.fl_str_mv	Artículo de revista
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dc.relation.references.none.fl_str_mv	Alcántara-Durán, J., Moreno-González, D., Gilbert-López, B., Molina-Díaz, A., & García-Reyes, J. (2018). Matrix-effect free multi-residue analysis of veterinary drugs in food samples of animal origin by nanoflow liquid chromatography high resolution mass spectrometry. Food Chemistry, 245, 29-38. http://dx.doi.org/10.1016/j. foodchem.2017.10.083 Amiri, A., & Ghaemi, F. (2017). Microextraction in packed syringe by using a threedimensional carbon nanotube/carbon nanofiber–graphene nanostructure coupled to dispersive liquid-liquid microextraction for the determination of phthalate esters in water samples. Microchimica Acta, 184(10), 3851-3848. https://doi.org/10.1007/s00604- 017-2416-8 Angulo, D., Andrade, R., Santos, R., Carneiro, B., Avellar, F., & Bastos, K. (2018). Pipettetip solid-phase extraction using polypyrrole as efficient adsorbent for extraction of avermectins and milbemycins in milk. Analytical and Bioanalytical Chemistry, 410(14), 3361-3374. https://doi.org/10.1007/s00216-018-1031-9 Bostan, I., Beloiu, R., & Bizon, N. (2015). Aprendiendo divisores digitales de frecuencia a través de actividades prácticas de laboratorio. Procedia - Social and Behavioral Sciences, 180, 1014-1021. https://doi.org/10.1016/j.sbspro.2015.02.195 Chen, W., Shah, U., & Brechtelsbauer, C. (2016). The discovery laboratory – A studentcentred experiential learning practical: Part I – Overview. Education for Chemical Engineers, 17, 44-53. https://doi.org/10.1016/j.ece.2016.07.005 Chiesa, L., Nobile, M., Biolatti, B., Pavlovic, R., Panseri, S., Cannizzo, F., & Arioli, F. (2016). Detection of selected corticosteroids and anabolic steroids in calf milk replacers by liquid chromatography-electrospray ionization-tandem mass spectrometry. Food Control, 61, 196-203. http://dx.doi.org/10.1016/j.foodcont.2015.09.028 Dănescu, E. (2015). Intercultural Education from the Perspective of Training Didactic Competences. Procedia - Social and Behavioral Sciences, 180, 537-542. https://doi. org/10.1016/j.sbspro.2015.02.156 Dönmez, N., & Ayas, A. (2010). Common misconceptions in nuclear chemistry unit. Procedia -Social and Behavioral Sciences, 2(2)1432-1436. Franco, R., Velasco, M., & Riveros, C. (2017). Los trabajos prácticos de laboratorio en la enseñanza de las ciencias: tendencias en revistas especializadas: 2012-2016. Tecné, Episteme y Didaxis, TED, (41), 37-56. Gañán, J., Morante-Zarcero, S., Pérez-Quintanilla, D., Marina, M., & Sierra, I. (2016). One-pot synthesized functionalized mesoporous silica as a reversed-phase sorbent for solidphase extraction of endocrine disrupting compounds in milks. Journal of Chromatography A, 1428, 228-235. http://dx.doi.org/10.1016/j.chroma.2015.08.063 Ghibaudi, E., Roletto, E., & Regis, A. (2016). Didattica della chimica e trasposizione didattica. Parte prima – I fondamenti teorici di una prassi. Perspectives in Science, 10, 19-27. https://doi.org/10.1016/j.pisc.2016.03.010 Hassan, E., Talbi, M., & Radid, M. (2015). Teaching and Learning of Experimental Science: The Case of Chemistry in Secondary Qualifying Morocco. Procedia - Social and Behavioral Sciences, 191, 2246-2249. https://doi.org/10.1016/j.sbspro.2015.04.338 Hernández, G. (2012). Enseñanza experimental. ¿Cómo y para qué? Educación Química, 23, 92-95. Jiang, Y., Ma, P., Li, X., Piao, H., Li, D., Sun, Y., Wang, X., & Song, D. (2018). Application of metalorganic framework MIL-101(Cr) tomicroextraction in packed syringe for determination of triazineherbicides in corn samples by liquid chromatography-tandem mass spectrometry. Journal of Chromatography A, 1574, 36-41. https://doi.org/10.1016/j. chroma.2018.09.008 Kampelmann, S., Kaethler, M., & Vickery, A. (2018). Curating complexity: An artful approach for real-world system transitions. Environmental Innovation and Societal Transitions, 27, 59-71. https://doi.org/10.1016/j.eist.2017.10.005 Li, N., Yang, X., Nian, L., Wang, Z., Lei, L., Wang, K., Zhang, H., Yu, A., & Zhang, Z. (2015). Determination of steroid hormones in milk using aqueous two-phase extraction coupled to liquid chromatography. Analytical Methods, 7(6), 2514-2522. https://doi.org/10.1039/ c4ay03036b Liu, H., Lin, T., Cheng, X., Li, N., Wang, L., & Li, Q. (2017). Simultaneous determination of anabolic steroids and β-agonists in milk by QuEchERS and ultra-high performance liquid chromatography tandem mass spectrometry. Journal of Chromatography B, 1043, 176-186. http://dx.doi.org/10.1016/j.jchromb.2016.08.016 Nacimento do, T., Avellar, F., Carneiro, B., & Bastos, K. (2018). Efficient removal of antiinflammatory phenylbutazone from an aqueous solution employing a composite material based on poly(aniline-co-pyrrole)/multi-walled carbon nanotubes. New Journal of Chemistry, 42(9), 7030-7042. https://doi.org/10.1039/c8nj00861b Nezhadali, A., Es’haghi, Z., & Khatibi, A. (2016). Selective extraction of progesterone hormones from environmental and biological samples using a polypyrrole molecularly imprinted polymer and determination by gas chromatography. Analytical Methods, 8(8), 1813-1827. https://doi.org/10.1039/c5ay02174j Özmen, H., Demirciog˘lu, H., & Demirciog˘lu, G. (2009). The effects of conceptual change texts accompanied with animations on overcoming 11th grade students’ alternative conceptions of chemical bonding. Computers & Education, 52, 681-695. Pelit, F., Pelit, L., Dizdaş, T., Aftafa, C., Ertaş, H., Yalçınkaya, E., Türkmen, H., & Ertaş, F. (2015). A novel polythiophene – ionic liquid modified clay composite solid phase microextraction fiber: preparation, characterization and application to pesticide analysis. Analytica Chimica Acta, 859, 37-45. http://dx.doi.org/10.1016/j.aca.2014.12.043 Ponzetto, F., Boccard, J., Baume, N., Kuuranne, T., Rudaz, S., Saugy, M., & Nicoli, R. (2017). High-resolution mass spectrometry as an alternative detection method to tandem mass spectrometry for the analysis of endogenous steroids in serum. Journal of Chromatography B, 1052, 34-42. http://dx.doi.org/10.1016/j.jchromb.2017.03.016 Qing, Z., Nia, S., & Hong, T. (2010). Developing critical thinking disposition by task-based learning in chemistry experiment teaching. Procedia - Social and Behavioral Sciences, 2, 4561-4570. Razmkhah, K., Sereshti, H., Soltani, S., & Nodeh, H. (2018). Extraction and determination of three steroid molecules in milk using functionalized magnetic carbon nanotubebased solid phase extraction coupled with HPLC. Food Analytical Methods, 11(11), 3179-3189. https://doi.org/10.1007/s12161-018-1298-7 Rojas-Hernández, A., & Ramírez-Silva, M. (2012). La enseñanza experimental de la Química General y la Química Analítica desde México (la Enep-Cuautitlán de la Unam y la Uam- Iztapalapa) en el último cuarto del siglo xx. Educación química, 23, 136-140 Sevian, H., & Fulmer, G. (2012). Student Outcomes from Innovations in Undergraduate Chemistry Laboratory Learning. Educación Química, 23, 149-161. Sudhoff, M., Prinza, C., & Kuhlenkötter, B. (2020). A Systematic Analysis of Learning Factories in Germany - Concepts, Production Processes, Didactics. Procedia Manufacturing, 45, 114-120. https://doi.org/10.1016/j.promfg.2020.04.081 Supasorn, S. (2012). Enhancing undergraduates’ conceptual understanding of organic acid-base-neutral extraction using inquiry-based experiments. Procedia - Social and Behavioral Sciences, 46, 4643-4650. Yang, L., Said, R., & Abdel-Rehim, M. (2017). Sorbent, device, matrix and application in microextraction by packed sorbent (MEPS): a review. Journal of Chromatography B, 1043, 33-43. https://doi.org/10.1016/j.jchromb.2016.10.044
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dc.relation.ispartofjournal.spa.fl_str_mv	Praxis & Saber
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dc.relation.citationedition.spa.fl_str_mv	Núm. 31 , Año 2021 : Investigación y pedagogía
dc.rights.none.fl_str_mv	Diego Hernando Angulo, Jaime Augusto Casas, Edna Carolina Cipagauta, David Eduardo Aparicio - 2021
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spelling	Angulo, Diego HernandoCasas, Jaime AugustoCipagauta, Edna CarolinaAparicio, David Eduardo2021-01-14 00:00:002026-04-16T17:39:47Z2021-01-14 00:00:002021-01-142216-0159https://repositorio.uptc.edu.co/handle/001/2116010.19053/22160159.v12.n31.2021.112152462-8603https://doi.org/10.19053/22160159.v12.n31.2021.11215text/xmlapplication/pdftext/htmlapplication/epub+zipUniversidad Pedagógica y Tecnológica de ColombiaDiego Hernando Angulo, Jaime Augusto Casas, Edna Carolina Cipagauta, David Eduardo Aparicio - 2021http://creativecommons.org/licenses/by-nc/4.0info:eu-repo/semantics/openAccessEsta obra está bajo una licencia internacional Creative Commons Atribución-NoComercial 4.0.http://purl.org/coar/access_right/c_abf2https://revistas.uptc.edu.co/index.php/praxis_saber/article/view/11215Experimental science didacticsLaboratory practical trainingSample preparationSPEHPLCDidáctica de las ciencias experimentalesTrabajos prácticos de laboratorioPreparación de muestrasDidática das ciências experimentaisPrática laboratorialPreparação de amostrasIntervención didáctica para la extracción y cuantificación de esteroides en orinaArtículo de revistahttp://purl.org/coar/resource_type/c_6501http://purl.org/coar/resource_type/c_2df8fbb1info:eu-repo/semantics/articleJournal articleinfo:eu-repo/semantics/publishedVersionTexthttp://purl.org/coar/version/c_970fb48d4fbd8a85Alcántara-Durán, J., Moreno-González, D., Gilbert-López, B., Molina-Díaz, A., & García-Reyes, J. (2018). Matrix-effect free multi-residue analysis of veterinary drugs in food samples of animal origin by nanoflow liquid chromatography high resolution mass spectrometry. Food Chemistry, 245, 29-38. http://dx.doi.org/10.1016/j. foodchem.2017.10.083Amiri, A., & Ghaemi, F. (2017). Microextraction in packed syringe by using a threedimensional carbon nanotube/carbon nanofiber–graphene nanostructure coupled to dispersive liquid-liquid microextraction for the determination of phthalate esters in water samples. Microchimica Acta, 184(10), 3851-3848. https://doi.org/10.1007/s00604- 017-2416-8Angulo, D., Andrade, R., Santos, R., Carneiro, B., Avellar, F., & Bastos, K. (2018). Pipettetip solid-phase extraction using polypyrrole as efficient adsorbent for extraction of avermectins and milbemycins in milk. Analytical and Bioanalytical Chemistry, 410(14), 3361-3374. https://doi.org/10.1007/s00216-018-1031-9Bostan, I., Beloiu, R., & Bizon, N. (2015). Aprendiendo divisores digitales de frecuencia a través de actividades prácticas de laboratorio. Procedia - Social and Behavioral Sciences, 180, 1014-1021. https://doi.org/10.1016/j.sbspro.2015.02.195Chen, W., Shah, U., & Brechtelsbauer, C. (2016). The discovery laboratory – A studentcentred experiential learning practical: Part I – Overview. Education for Chemical Engineers, 17, 44-53. https://doi.org/10.1016/j.ece.2016.07.005Chiesa, L., Nobile, M., Biolatti, B., Pavlovic, R., Panseri, S., Cannizzo, F., & Arioli, F. (2016). Detection of selected corticosteroids and anabolic steroids in calf milk replacers by liquid chromatography-electrospray ionization-tandem mass spectrometry. Food Control, 61, 196-203. http://dx.doi.org/10.1016/j.foodcont.2015.09.028Dănescu, E. (2015). Intercultural Education from the Perspective of Training Didactic Competences. Procedia - Social and Behavioral Sciences, 180, 537-542. https://doi. org/10.1016/j.sbspro.2015.02.156Dönmez, N., & Ayas, A. (2010). Common misconceptions in nuclear chemistry unit. Procedia -Social and Behavioral Sciences, 2(2)1432-1436.Franco, R., Velasco, M., & Riveros, C. (2017). Los trabajos prácticos de laboratorio en la enseñanza de las ciencias: tendencias en revistas especializadas: 2012-2016. Tecné, Episteme y Didaxis, TED, (41), 37-56.Gañán, J., Morante-Zarcero, S., Pérez-Quintanilla, D., Marina, M., & Sierra, I. (2016). One-pot synthesized functionalized mesoporous silica as a reversed-phase sorbent for solidphase extraction of endocrine disrupting compounds in milks. Journal of Chromatography A, 1428, 228-235. http://dx.doi.org/10.1016/j.chroma.2015.08.063Ghibaudi, E., Roletto, E., & Regis, A. (2016). Didattica della chimica e trasposizione didattica. Parte prima – I fondamenti teorici di una prassi. Perspectives in Science, 10, 19-27. https://doi.org/10.1016/j.pisc.2016.03.010Hassan, E., Talbi, M., & Radid, M. (2015). Teaching and Learning of Experimental Science: The Case of Chemistry in Secondary Qualifying Morocco. Procedia - Social and Behavioral Sciences, 191, 2246-2249. https://doi.org/10.1016/j.sbspro.2015.04.338Hernández, G. (2012). Enseñanza experimental. ¿Cómo y para qué? Educación Química, 23, 92-95.Jiang, Y., Ma, P., Li, X., Piao, H., Li, D., Sun, Y., Wang, X., & Song, D. (2018). Application of metalorganic framework MIL-101(Cr) tomicroextraction in packed syringe for determination of triazineherbicides in corn samples by liquid chromatography-tandem mass spectrometry. Journal of Chromatography A, 1574, 36-41. https://doi.org/10.1016/j. chroma.2018.09.008Kampelmann, S., Kaethler, M., & Vickery, A. (2018). Curating complexity: An artful approach for real-world system transitions. Environmental Innovation and Societal Transitions, 27, 59-71. https://doi.org/10.1016/j.eist.2017.10.005Li, N., Yang, X., Nian, L., Wang, Z., Lei, L., Wang, K., Zhang, H., Yu, A., & Zhang, Z. (2015). Determination of steroid hormones in milk using aqueous two-phase extraction coupled to liquid chromatography. Analytical Methods, 7(6), 2514-2522. https://doi.org/10.1039/ c4ay03036bLiu, H., Lin, T., Cheng, X., Li, N., Wang, L., & Li, Q. (2017). Simultaneous determination of anabolic steroids and β-agonists in milk by QuEchERS and ultra-high performance liquid chromatography tandem mass spectrometry. Journal of Chromatography B, 1043, 176-186. http://dx.doi.org/10.1016/j.jchromb.2016.08.016Nacimento do, T., Avellar, F., Carneiro, B., & Bastos, K. (2018). Efficient removal of antiinflammatory phenylbutazone from an aqueous solution employing a composite material based on poly(aniline-co-pyrrole)/multi-walled carbon nanotubes. New Journal of Chemistry, 42(9), 7030-7042. https://doi.org/10.1039/c8nj00861bNezhadali, A., Es’haghi, Z., & Khatibi, A. (2016). Selective extraction of progesterone hormones from environmental and biological samples using a polypyrrole molecularly imprinted polymer and determination by gas chromatography. Analytical Methods, 8(8), 1813-1827. https://doi.org/10.1039/c5ay02174jÖzmen, H., Demirciog˘lu, H., & Demirciog˘lu, G. (2009). The effects of conceptual change texts accompanied with animations on overcoming 11th grade students’ alternative conceptions of chemical bonding. Computers & Education, 52, 681-695.Pelit, F., Pelit, L., Dizdaş, T., Aftafa, C., Ertaş, H., Yalçınkaya, E., Türkmen, H., & Ertaş, F. (2015). A novel polythiophene – ionic liquid modified clay composite solid phase microextraction fiber: preparation, characterization and application to pesticide analysis. Analytica Chimica Acta, 859, 37-45. http://dx.doi.org/10.1016/j.aca.2014.12.043Ponzetto, F., Boccard, J., Baume, N., Kuuranne, T., Rudaz, S., Saugy, M., & Nicoli, R. (2017). High-resolution mass spectrometry as an alternative detection method to tandem mass spectrometry for the analysis of endogenous steroids in serum. Journal of Chromatography B, 1052, 34-42. http://dx.doi.org/10.1016/j.jchromb.2017.03.016Qing, Z., Nia, S., & Hong, T. (2010). Developing critical thinking disposition by task-based learning in chemistry experiment teaching. Procedia - Social and Behavioral Sciences, 2, 4561-4570.Razmkhah, K., Sereshti, H., Soltani, S., & Nodeh, H. (2018). Extraction and determination of three steroid molecules in milk using functionalized magnetic carbon nanotubebased solid phase extraction coupled with HPLC. Food Analytical Methods, 11(11), 3179-3189. https://doi.org/10.1007/s12161-018-1298-7Rojas-Hernández, A., & Ramírez-Silva, M. (2012). La enseñanza experimental de la Química General y la Química Analítica desde México (la Enep-Cuautitlán de la Unam y la Uam- Iztapalapa) en el último cuarto del siglo xx. Educación química, 23, 136-140Sevian, H., & Fulmer, G. (2012). Student Outcomes from Innovations in Undergraduate Chemistry Laboratory Learning. Educación Química, 23, 149-161.Sudhoff, M., Prinza, C., & Kuhlenkötter, B. (2020). A Systematic Analysis of Learning Factories in Germany - Concepts, Production Processes, Didactics. Procedia Manufacturing, 45, 114-120. https://doi.org/10.1016/j.promfg.2020.04.081Supasorn, S. (2012). Enhancing undergraduates’ conceptual understanding of organic acid-base-neutral extraction using inquiry-based experiments. Procedia - Social and Behavioral Sciences, 46, 4643-4650.Yang, L., Said, R., & Abdel-Rehim, M. (2017). Sorbent, device, matrix and application in microextraction by packed sorbent (MEPS): a review. Journal of Chromatography B, 1043, 33-43. https://doi.org/10.1016/j.jchromb.2016.10.044e1121531e1121512Praxis & Saberhttps://revistas.uptc.edu.co/index.php/praxis_saber/article/download/11215/12588https://revistas.uptc.edu.co/index.php/praxis_saber/article/download/11215/10446https://revistas.uptc.edu.co/index.php/praxis_saber/article/download/11215/10447https://revistas.uptc.edu.co/index.php/praxis_saber/article/download/11215/10448Núm. 31 , Año 2021 : Investigación y pedagogíaPublicationOREORE.xmltext/xml2765https://repositorio.uptc.edu.co/bitstreams/560ecee4-9965-4d9e-baad-de7aabbabb4f/download7daa3836a367443e6267e4b9a2586fa4MD51falseAnonymousREAD001/21160oai:repositorio.uptc.edu.co:001/211602026-09-29 12:54:33.788http://creativecommons.org/licenses/by-nc/4.0metadata.onlyhttps://repositorio.uptc.edu.coRepositorio Institucional UPTCbdigital@metabiblioteca.com

Intervención didáctica para la extracción y cuantificación de esteroides en orina

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